1.1 This practice is an alternative method to Test Method C698 for the determination of the oxygen-to-metal atom ratio (O/M) in sintered mixed oxide fuel (MOX) pellets. The method presented in Test Method C698 is a one-step thermogravimetric method for determining O/M ratio in sintered MOX powders and pellets. As stated in Test Method C698, thermogravimetric methods using a two-step heating cycle are also satisfactory (1, 2).2 The method presented in this test method is a two-step heating cycle method. This test method is applicable to sintered MOX pellets containing up to 10 weight percent PuO2.
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- Published:
- 06/01/2015
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