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1.1 This practice covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis.

1.2 Reduction and division procedures are prescribed for coals of the following groups:

1.2.1 Group A includes coals that have been cleaned in all sizes.

1.2.2 Group B includes all other coals. Unknown coals are to be considered under Group B.

1.2.3 Group A allows smaller weight laboratory samples to be retained than Group B. These lower weights may be used for particular coals if they have been shown, by using the procedures of Annex A1.2, to give a sample preparation and analysis variance which is no more than 20 % of the total analysis variance.

1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Published:
04/01/2012
Number of Pages:
12
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Other standards are used to collect the gross sample: Practice D2234/D2234M allows for one division of the gross sample before crushing. The mass and top size of the gross or divided sample collected by using these guides and practices are usually too large for chemical or physical testing. Practice D2013 provides instructions for reducing and dividing the gross or divided sample, by on-line or off-line processes, or both, to a top size and mass suitable to the performance of testing. Any bias in the gross or divided sample before adherence to this practice will remain in the final sample resulting from use of this practice. Therefore, carefully select the standard to be used to collect the gross sample.

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Published:
09/01/2018
Number of Pages:
12
File Size:
1 file , 480 KB