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1.1 These test methods cover the chemical analysis of carbon steels, low-alloy steels, silicon electrical steels, ingot iron, and wrought iron having chemical compositions within the following limits:

Element Composition Range, %
Aluminum 0.001 to 1.50
Antimony 0.002 to 0.03
Arsenic 0.0005 to 0.10
Bismuth 0.005 to 0.50
Boron 0.0005 to 0.02
Calcium 0.0005 to 0.01
Cerium 0.005 to 0.50
Chromium 0.005 to 3.99
Cobalt 0.01 to 0.30
Columbium (Niobium) 0.002 to 0.20
Copper 0.005 to 1.50
Lanthanum 0.001 to 0.30
Lead 0.001 to 0.50
Manganese 0.01 to 2.50
Molybdenum 0.002 to 1.50
Nickel 0.005 to 5.00
Nitrogen 0.0005 to 0.04
Oxygen 0.0001 to 0.03
Phosphorus 0.001 to 0.25
Selenium 0.001 to 0.50
Silicon 0.001 to 5.00
Sulfur 0.001 to 0.60
Tin 0.002 to 0.10
Titanium 0.002 to 0.60
Tungsten 0.005 to 0.10
Vanadium 0.005 to 0.50
Zirconium 0.005 to 0.15

1.2 The test methods in this standard are contained in the sections indicated as follows:

Sections
Aluminum, Total, by the 8-Quinolinol Gravimetric Method
(0.20 % to 1.5 %)
124131
Aluminum, Total, by the 8-Quinolinol Spectrophotometric
Method (0.003 % to 0.20 %)
7686
Aluminum, Total or Acid-Soluble, by the Atomic Absorption
Spectrometry Method (0.005 % to 0.20 %)
308317
Antimony by the Brilliant Green Spectrophotometric
Method (0.0002 % to 0.030 %)
142151
Bismuth by the Atomic Absorption Spectrometry
Method (0.02 % to 0.25 %)
298307
Boron by the Distillation-Curcumin Spectrophotometric
Method (0.0003 % to 0.006 %)
208219
Calcium by the Direct-Current Argon Plasma Atomic
Emission Spectroscopy Method (0.0005 % to 0.010 %)
289297
Carbon, Total, by the Combustion Gravimetric Method
(0.05 % to1.80 %)-Discontinued 1995
Cerium and Lanthanum by the Direct Current Plasma
Atomic Emission Spectrometry Method
(0.003 % to 0.50 % Cerium, 0.001 % to 0.30 % Lanthanum)
249257
Chromium by the Atomic Absorption Spectrometry
Method (0.006 % to 1.00 %)
220229
Chromium by the Peroxydisulfate Oxidation-Titration
Method (0.05 % to 3.99 %)
230238
Cobalt by the Nitroso-R Salt Spectrophotometric
Method (0.01 % to 0.30 %)
5362
Copper by the Atomic Absorption Spectrometry
Method (0.004 % to 0.5 %)
279288
Copper by the Neocuproine Spectrophotometric
Method (0.005 % to 1.50 %)
114123
Lead by the Ion-Exchange-Atomic Absorption Spectrometry
Method (0.001 % to 0.50 %)
132141
Manganese by the Atomic Absorption Spectrometry
Method (0.005 % to 2.0 %)
269278
Manganese by the Metaperiodate Spectrophotometric
Method (0.01 % to 2.5 %)
9-18
Manganese by the Peroxydisulfate-Arsenite Titrimetric
Method(0.10 % to 2.50 %)
164171
Molybdenum by the Thiocyanate Spectrophotometric
Method (0.01 % to 1.50 %)
152163
Nickel by the Atomic Absorption Spectrometry
Method (0.003 % to 0.5 %)
318327
Nickel by the Dimethylglyoxime Gravimetric
Method (0.1 % to 5.00 %)
180187
Nickel by the Ion-Exchange-Atomic-Absorption Spectrometry
Method (0.005 % to 1.00 %)
188197
Phosphorus by the Alkalimetric Method
(0.02 % to 0.25 %)
172179
Phosphorus by the Molybdenum Blue Spectrophotometric
Method (0.003 % to 0.09 %)
19-30
Silicon by the Molybdenum Blue Spectrophotometric
Method (0.01 % to 0.06 %)
103113
Silicon by the Gravimetric Titration
Method (0.05 % to 3.5 %)
4652
Sulfur by the Combustion-Iodate Titration Method
(0.005 % to 0.3 %)
3745
Tin by the Sulfide-Iodometric Titration
Method (0.01 % to 0.1 %)
95102
Tin by the Solvent Extraction-Atomic Absorption Spectrometry Method
(0.002 % to 0.10 %)
198207
Titanium, Total, by the Diantipyrylmethane Spectrophotometric
Method (0.025 % to 0.30 %)
258268
Vanadium by the Atomic Absorption Spectrometry
Method (0.006 % to 0.15 %)
239248

1.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E1019.

1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in are also used.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special Warning paragraphs throughout these test methods.

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Published:
08/15/2012
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